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العنوان
Studies on metal complexes of some transition metal ions with some hydrazide derivatives /
المؤلف
Zaky, Rania Ramadan.
هيئة الاعداد
باحث / رانيا رمضان زكى
مشرف / كمال محمد احمد ابراهيم
مشرف / جابر محمد ابوالريش
مشرف / رأفت السيد منصور الشاذلى
الموضوع
Inorganic Chemistry. Hydrazones complexes.
تاريخ النشر
2006.
عدد الصفحات
243 p. :
اللغة
الإنجليزية
الدرجة
الدكتوراه
التخصص
الكيمياء
تاريخ الإجازة
1/1/2006
مكان الإجازة
جامعة المنصورة - كلية العلوم - Department of Chemistry
الفهرس
Only 14 pages are availabe for public view

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Abstract

The work described in this thesis has been undertaken with the aim of searching for synthesis of new hydrazone complexes. The work presented in this thesis consists of three main parts.
Part I : Introduction It contains a literature survey on the hydrazone complexes which have been prepared up tp 2006 and its application in analytical chemistry and biological activity.
Part II : Experimental It contains a description of the experimental procedures used for the preparation of the hydrazones from the reaction of 3­hydroxy ­2­naphthoic hydrazide and different ketones and/or aldehydes and its complexes Part III : Results and Discussion It contains a the results obtained and a discussion of this results in order to determned the chemical structures of the isolated ligands (hydrazones) and its metal complexes using different chemical analysis methods like spectral data (IR, UV­Vis, H­NMR, ESR), thermal, magnetic measurements. Also, the antimicrobial activities for many prepared compounds was performed using the cup­diffusion technique in solid agar plates against two important microbes. Pseudomonas aeurginosa was tested as a standard gram negative pathogenic bacteria and Bacillus Subtilis as standard gram positive bacteria.