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العنوان
Synthesis of graphene and graphene oxide by microwave plasma and reduction of graphene oxide using laser /
الناشر
Mahmoud Gomaa Mahmoud Habieb ,
المؤلف
Mahmoud Gomaa Mahmoud Habieb
هيئة الاعداد
باحث / Mahmoud Gomaa Mahmoud Habieb
مشرف / Gamal Abdelfattah Ali
مناقش / Gamal Abdelfattah Ali
مناقش / Mahmoud Gomaa Mahmoud Habieb
تاريخ النشر
2016
عدد الصفحات
118 P. :
اللغة
الإنجليزية
الدرجة
ماجستير
التخصص
الفيزياء والفلك (المتنوعة)
تاريخ الإجازة
6/3/2017
مكان الإجازة
جامعة القاهرة - المعهد القومى لعلوم الليزر - Laser Science and Interactions
الفهرس
Only 14 pages are availabe for public view

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Abstract

All the previous studies have been reviewed only the synthesis of graphene by microwave plasma chemical vapor deposition technique, but no study has been reviewed the synthesis of graphene oxide by (MWPCVD) technique. In this thesis, a simple experiment was constructed for rapid synthesize of graphene and graphene oxide (GO) sheets simultaneously using microwave plasma chemical vapor deposition (MWPCVD) technique, which uses a microwave source (magnetron) operating at a frequency of 2.45 GHZ and a power of 700W to produce plasma inside a tube of quartz. The high-density polyethylene which consists of small beads was used as a carbon source. The graphene and graphene oxide were deposited after the quartz tube was evacuated by a rotary pump for 30 min and exposed to microwave irradiation with a power of 700W for 2 minutes. The graphene and graphene oxide sheets were characterized by different techniques such as transmission electron microscopy (TEM), X-ray diffraction, Raman spectroscopy, UV-Visible spectroscopy, Spectrofluorometer and FT-IR spectroscopy. TEM showed that the morphology of graphene suspension sheets are not perfectly flat but exhibit crumpled and folded. X-ray diffraction for graphene showed that the presence of a high and small peak around 2k = 24.56{u00BA} and 2k= 43.65{u00BA} respectively, which indicated that graphene has an amorphous carbon structure. Raman spectra indicated the difference between position and shape of peaks, crystal size and intensity ratio of the D to G modes (ID/IG) for graphene and graphene oxide