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العنوان
Synthesis And characterization Of Super Paramagnetic Nanoparticles Functionalized With Sulphonamide Imine For Heavy Metals Determination =
المؤلف
Ali, Eslam Saeed Abu-Elsoud Hussien.
هيئة الاعداد
مشرف / Eslam Saeed Abu-Elsoud Hussien Ali
مشرف / Ali El Dissouky
مشرف / Amel Fawzy El Husseiny
مشرف / Gamal Badee Mohamed
الموضوع
Nanoparticles. Metals.
تاريخ النشر
2015.
عدد الصفحات
177 p. :
اللغة
الإنجليزية
الدرجة
ماجستير
التخصص
الكيمياء
تاريخ الإجازة
9/6/2015
مكان الإجازة
جامعة الاسكندريه - كلية العلوم - Chemistry
الفهرس
Only 14 pages are availabe for public view

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Abstract

In this work a series of sulphonamide imine ligands (HL1-5) were prepared by the condensation of the triple sulpha drugs namely (Sulfamethazine, Sulfamerazine and Sulfadiazine) with salicylaldehyde and 2-hydroxy1-naphthaldehyde. Direct reactions with copper acetate dihydrate and zinc acetate dihydrate furnished the corresponding complexes in good yields. The structures of the ligands and their metal complexes were fully characterized using elemental analysis, molar conductance, spectroscopic measurements (FT-IR, UV-vis, 1HNMR, Fluorescence, EPR and mass spectra), magnetic susceptibility and thermal studies.