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Abstract The present work, an electrochemical sensor based on electrochemical reduced graphine oxide modified glassy carbon electrode (GCE) was used for simultaneous determination of gallic (GA) and protocatechuic (PA) acids. The prepared sensor shows a significant enhancement in electro catalytic performance for the two acids. A good resolution of their voltammetry peaks was obtained, and a square wave voltammetr ic method was applied for the simultaneous detection of GA and PA in their mixture. In the second part of work, using ß -Cyclodextrin and Multi-Walled Carbon nanotube with reduced graphene oxide (ß -CD/ MWCNTs/rGO ) illustrate a high and more sensitive electrode than rGO only. The novel electrochemical sensor (ß -CD/ MWCNTs/rGO ) fabricated by electropolymarization of ß - cyclodextrin on MWCNTs/rGO/GCE modified electrode.The coated β-CD polymer had high electrical. |